Mn₂(CO)9As(C₆H₅)3

Base Information

Chemical Name:Mn₂(CO)9As(C₆H₅)3
CAS No.:75039-06-4
Molecular Formula:C₂₇H₁₅AsMn₂O₉
Molecular Weight:668.208
Hs Code.:

Mn<sub>2</sub>(CO)9As(C<sub>6</sub>H<sub>5</sub>)3

Synonyms:Mn₂(CO)9As(C₆H₅)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Mn₂(CO)9As(C₆H₅)3

Chemical Property:

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Technology Process of Mn₂(CO)9As(C₆H₅)3

There total 3 articles about Mn₂(CO)9As(C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10170-69-1
dimanganese decacarbonyl

: 603-32-7
triphenyl-arsane

: 74-95-3
1,1-dibromomethane

: 14516-54-2
bromopentacarbonylmanganese(I)

: 75039-06-4
Mn₂(CO)9As(C₆H₅)3

: 14841-06-6
Mn(CO)4As(C₆H₅)3Br

Guidance literature:: In hexane; Irradiation (UV/VIS); irradn. (366 nm) of hexane soln. of Mn2(CO)10, CH2Br2 (0.1 M), and AsPh3 (1.9E-3 to 1.0E-2 M) at 0°C; not isolated; detected by IR; Kinetics;
DOI:10.1021/ja00306a016

Reference yield:

: 16972-33-1
pentacarbonylhydridomanganese

: 603-32-7
triphenyl-arsane

: HMn(CO)4As(C₆H₅)3

: 75039-06-4,75081-79-7
cis-nonacarbonyl(triphenylarsane)dimanganese

: 75039-06-4,75081-79-7
trans-nonacarbonyl(triphenylarsane)dimanganese

Guidance literature:: With oxygen; In Petroleum ether; byproducts: CH2O; complex mixed at -10°C with ligand soln., stirred for hours under air; filtered, chromd. (SiO2, petroleum ether, toluene/petroleum ether), recrystd. (petroleum ether at -80°C); elem. anal.;
DOI:10.1016/S0022-328X(00)81230-9

Reference yield:

: 16972-33-1
pentacarbonylhydridomanganese

: 603-32-7
triphenyl-arsane

: HMn(CO)4As(C₆H₅)3

: 75039-06-4,75081-79-7
cis-nonacarbonyl(triphenylarsane)dimanganese

: 75039-06-4,75081-79-7
trans-nonacarbonyl(triphenylarsane)dimanganese

Guidance literature:: With oxygen; In Petroleum ether; byproducts: CH2O; complex mixed at -10°C with ligand soln., stirred for hours under air; filtered, chromd. (SiO2, petroleum ether, toluene/petroleum ether), recrystd. (petroleum ether at -80°C); elem. anal.;
DOI:10.1016/S0022-328X(00)81230-9