4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile

Base Information

Chemical Name:4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile
CAS No.:1596293-20-7
Molecular Formula:C₂₃H₁₉N₃O₂
Molecular Weight:369.423
Hs Code.:

Synonyms:4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile

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Chemical Property of 4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile

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Technology Process of 4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile

There total 1 articles about 4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1195-59-1
2.6-bis(hydroxymethyl)pyridine

: 17201-43-3
4-cyanobenzyl bromide

: 1596293-20-7
4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 70 ℃; for 48h; Inert atmosphere;
DOI:10.1021/jacs.5b09738

Reference yield: 90.0%

: 1596293-20-7
4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile

: 1609137-34-9
C₂₃H₂₇N₃O₂

Guidance literature:: With borane-THF; In tetrahydrofuran; at 20 - 70 ℃; for 20h; Inert atmosphere; Cooling with ice;
DOI:10.1021/jacs.5b09738

Reference yield:

: 1596293-20-7
4,4'-(((pyridine-2,6-diylbis(methylene))bis(oxy))bis(methylene))dibenzonitrile

: 1609137-36-1
C₃₀H₃₂N₄O₂*C₂₉H₄₄N₂O

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 16 h / Reflux

2.1: sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate / chloroform / 43 h / 50 °C

2.2: 20 °C

With borane-THF; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In tetrahydrofuran; chloroform;
DOI:10.1002/chem.201400323