1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate

Base Information

Chemical Name:1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate
CAS No.:1335093-69-0
Molecular Formula:C₂H₂O₄*C₂₁H₂₂FNO₄
Molecular Weight:461.444
Hs Code.:

Synonyms:1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate

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Chemical Property of 1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate

Chemical Property:

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Technology Process of 1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate

There total 6 articles about 1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335093-53-2
1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline

: 144-62-7,97993-78-7
oxalic acid

: 1335093-69-0
1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate

Guidance literature:: In methanol; ethyl acetate; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.05.072

Reference yield:

: 1252658-33-5
2-(4-(benzyloxy)-3-methoxyphenyl)-N-(2-(3,4-dimethoxyphenyl)-2-hydroxyethyl)acetamide

: 1335093-69-0
1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / acetonitrile / 0.5 h / Reflux; Inert atmosphere

2: hydrogenchloride / ethanol; water / 2 h / Reflux; Inert atmosphere

3: potassium carbonate / acetone / Reflux; Inert atmosphere

4: methanol; ethyl acetate / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; potassium carbonate; trichlorophosphate; In methanol; ethanol; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2011.05.072

Reference yield:

: 15471-89-3
α-(aminomethyl)-3,4-dimethoxybenzyl alcohol hydrochloride

: 1335093-69-0
1-(4-(2-fluoroethoxy)-3-methoxybenzyl)-6,7-dimethoxyisoquinoline oxalate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / diethyl ether / 0.08 h / Inert atmosphere

1.2: 2 h / Inert atmosphere

2.1: trichlorophosphate / acetonitrile / 0.5 h / Reflux; Inert atmosphere

3.1: hydrogenchloride / ethanol; water / 2 h / Reflux; Inert atmosphere

4.1: potassium carbonate / acetone / Reflux; Inert atmosphere

5.1: methanol; ethyl acetate / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium carbonate; potassium carbonate; trichlorophosphate; In methanol; diethyl ether; ethanol; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2011.05.072