(S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate

Base Information

Chemical Name:(S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate
CAS No.:1354491-07-8
Molecular Formula:C₂₇H₃₆O₃
Molecular Weight:408.581
Hs Code.:

Synonyms:(S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate

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Chemical Property of (S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate

Chemical Property:

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Technology Process of (S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate

There total 9 articles about (S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 859217-67-7
2-(4,4-dimethylcyclohex-1-ene-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1354491-05-6
(S)-ethyl 2-tert-butoxy-2-(1-chloro-3-methylnaphthalen-2-yl)acetate

: 1354491-07-8
(S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate

Guidance literature:: With potassium dihydrogenphosphate; (2-dicyclohexyl-phosphino-2',6'-dimethoxy-1,1'-biphenyl)[2-(2-aminoethylphenyl)]palladium(II) chloride methyl-t-butyl ether adduct; In tetrahydrofuran; at 110 ℃; for 1h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 1322036-27-0
1-chloro-3-methyl-naphthalen-2-ol

: 1354491-07-8
(S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate

Guidance literature:: Multi-step reaction with 9 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 3 h / -78 °C

2.1: lithium chloride / bis-triphenylphosphine-palladium(II) chloride / 28 h / 50 - 80 °C / Inert atmosphere

3.1: (DHQ)₂PHAL / water; tert-butyl alcohol / 8 h / 0 °C

4.1: pyridine / dichloromethane / 19 h / 20 °C

5.1: perchloric acid / 1.5 h / 20 °C

5.2: 1 h

6.1: sodium hydroxide; methanol / tetrahydrofuran / 20 °C

7.1: chromium(VI) oxide; periodic acid / acetonitrile; water / 2 h / 0 °C

8.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

9.1: potassium dihydrogenphosphate / (2-dicyclohexyl-phosphino-2',6'-dimethoxy-1,1'-biphenyl)[2-(2-aminoethylphenyl)]palladium(II) chloride methyl-t-butyl ether adduct / tetrahydrofuran / 1 h / 110 °C / Inert atmosphere; Microwave irradiation

With pyridine; 2,6-dimethylpyridine; chromium(VI) oxide; methanol; potassium dihydrogenphosphate; perchloric acid; (DHQ)₂PHAL; caesium carbonate; periodic acid; lithium chloride; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; (2-dicyclohexyl-phosphino-2',6'-dimethoxy-1,1'-biphenyl)[2-(2-aminoethylphenyl)]palladium(II) chloride methyl-t-butyl ether adduct; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

Reference yield:

: 1354490-94-0
trifluoromethanesulfonic acid 1-chloro-3-methylnaphthalen-2-yl ester

: 1354491-07-8
(S)-ethyl 2-tert-butoxy-2-(1-(4,4-dimethylcyclohex-1-enyl)-3-methylnaphthalen-2-yl)acetate

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium chloride / bis-triphenylphosphine-palladium(II) chloride / 28 h / 50 - 80 °C / Inert atmosphere

2.1: (DHQ)₂PHAL / water; tert-butyl alcohol / 8 h / 0 °C

3.1: pyridine / dichloromethane / 19 h / 20 °C

4.1: perchloric acid / 1.5 h / 20 °C

4.2: 1 h

5.1: sodium hydroxide; methanol / tetrahydrofuran / 20 °C

6.1: chromium(VI) oxide; periodic acid / acetonitrile; water / 2 h / 0 °C

7.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

8.1: potassium dihydrogenphosphate / (2-dicyclohexyl-phosphino-2',6'-dimethoxy-1,1'-biphenyl)[2-(2-aminoethylphenyl)]palladium(II) chloride methyl-t-butyl ether adduct / tetrahydrofuran / 1 h / 110 °C / Inert atmosphere; Microwave irradiation

With pyridine; chromium(VI) oxide; methanol; potassium dihydrogenphosphate; perchloric acid; (DHQ)₂PHAL; caesium carbonate; periodic acid; lithium chloride; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; (2-dicyclohexyl-phosphino-2',6'-dimethoxy-1,1'-biphenyl)[2-(2-aminoethylphenyl)]palladium(II) chloride methyl-t-butyl ether adduct; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;