4-Methyl-2,7-diphenyl-1lambda4,8-dithia-2,3-diazabicyclo[3.3.0]octa-1(5),3,6-triene

Base Information

Chemical Name:4-Methyl-2,7-diphenyl-1lambda4,8-dithia-2,3-diazabicyclo[3.3.0]octa-1(5),3,6-triene
CAS No.:6450-60-8
Molecular Formula:C₁₄H₁₅N
Molecular Weight:197.28
Hs Code.:
DSSTox Substance ID:DTXSID00409695

Synonyms:6450-60-8;4-Methyl-2,7-diphenyl-1lambda4,8-dithia-2,3-diazabicyclo[3.3.0]octa-1(5),3,6-triene;AJ-797/37155021;DTXSID00409695;3-methyl-1,5-diphenyl-1H-7lambda~4~-[1,2]dithiolo[5,1-e][1,2,3]thiadiazole

Suppliers and Price of 4-Methyl-2,7-diphenyl-1lambda4,8-dithia-2,3-diazabicyclo[3.3.0]octa-1(5),3,6-triene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-Methyl-2,7-diphenyl-1lambda4,8-dithia-2,3-diazabicyclo[3.3.0]octa-1(5),3,6-triene

Chemical Property:

Density:1.33g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:310.05984080
Heavy Atom Count:21
Complexity:509

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NN(S2=C1C=C(S2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 4-Methyl-2,7-diphenyl-1lambda4,8-dithia-2,3-diazabicyclo[3.3.0]octa-1(5),3,6-triene

There total 5 articles about 4-Methyl-2,7-diphenyl-1lambda4,8-dithia-2,3-diazabicyclo[3.3.0]octa-1(5),3,6-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4657-93-6
5-aminoacenaphthene

: 74-88-4
methyl iodide

: 6450-60-8
5-dimethylaminoacenaphthene

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; at 20 - 70 ℃; for 2h;
DOI:10.1023/A:1022429322461

Reference yield:

: 602-87-9
4-nitroacenaphthene

: 6450-60-8
5-dimethylaminoacenaphthene

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂S₂O₄; diluted alcohol

2: sodium acetate; water / folgendes Erwaermen des Reaktionsgemisches auf 80grad

With sodium dithionite; ethanol; water; sodium acetate;