Technology Process of C35H48BIN4O12
There total 16 articles about C35H48BIN4O12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydrogencarbonate / acetone; water
2: N,N,N-trimethylbenzenemethanaminium dichloroiodate; sodium hydrogencarbonate / methanol; dichloromethane
3: potassium carbonate / acetone / 48 h / Reflux
4: trifluoroacetic acid / dichloromethane
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile
With
sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; N,N,N-trimethylbenzenemethanaminium dichloroiodate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;