C₂₉H₄₇NO₄Si

Base Information

Chemical Name:C₂₉H₄₇NO₄Si
CAS No.:1353674-71-1
Molecular Formula:C₂₉H₄₇NO₄Si
Molecular Weight:501.782
Hs Code.:

C<sub>29</sub>H<sub>47</sub>NO<sub>4</sub>Si

Synonyms:C₂₉H₄₇NO₄Si

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Chemical Property of C₂₉H₄₇NO₄Si

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Technology Process of C₂₉H₄₇NO₄Si

There total 7 articles about C₂₉H₄₇NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1353674-49-3
(2S,3R)-3-(tert-butyldimethylsilyloxy)-1-(4-(methoxymethoxy)phenyl)-N-methyl-N-((S)-1-phenylethyl)-6-(triisopropylsilyloxy)hexan-2-amine

: 1353674-71-1
C₂₉H₄₇NO₄Si

Guidance literature:: With pyridine; triethylamine hydrofluoride; for 26h; Inert atmosphere;
DOI:10.1021/ol202683k

Reference yield:

: 618884-71-2
(S)-N-methoxy-N-methyl-1-((S)-1-phenylethyl)aziridine-2-carboxamide

: 1353674-71-1
C₂₉H₄₇NO₄Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: tert.-butyl lithium / diethyl ether; pentane / 0.5 h / -78 °C / Inert atmosphere

1.2: 2.5 h / -78 - 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate; zinc(II) chloride / methanol / 0.5 h / -78 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: dmap / dichloromethane / 12 h / 0 °C / Inert atmosphere

4.1: 1,4-dioxane / 0.08 h / 20 °C / Inert atmosphere

5.1: copper(l) iodide / tetrahydrofuran; 1,4-dioxane / 0.17 h / 0 °C / Inert atmosphere

6.1: pyridine; triethylamine hydrofluoride / 26 h / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; copper(l) iodide; tert.-butyl lithium; triethylamine hydrofluoride; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; pentane;
DOI:10.1021/ol202683k

Reference yield:

: 1353674-47-1
C₂₃H₃₉NO₂Si

: 1353674-71-1
C₂₉H₄₇NO₄Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate; zinc(II) chloride / methanol / 0.5 h / -78 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: dmap / dichloromethane / 12 h / 0 °C / Inert atmosphere

3.1: 1,4-dioxane / 0.08 h / 20 °C / Inert atmosphere

4.1: copper(l) iodide / tetrahydrofuran; 1,4-dioxane / 0.17 h / 0 °C / Inert atmosphere

5.1: pyridine; triethylamine hydrofluoride / 26 h / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; copper(l) iodide; triethylamine hydrofluoride; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/ol202683k