phenyl(6,7,8,9-tetrahydro-5H-tetrazolo[1,5-a]azepin-9-yl)methyl acetate

Base Information

Chemical Name:phenyl(6,7,8,9-tetrahydro-5H-tetrazolo[1,5-a]azepin-9-yl)methyl acetate
CAS No.:926290-85-9
Molecular Formula:C₁₅H₁₈N₄O₂
Molecular Weight:286.334
Hs Code.:

Synonyms:phenyl(6,7,8,9-tetrahydro-5H-tetrazolo[1,5-a]azepin-9-yl)methyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl(6,7,8,9-tetrahydro-5H-tetrazolo[1,5-a]azepin-9-yl)methyl acetate

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Technology Process of phenyl(6,7,8,9-tetrahydro-5H-tetrazolo[1,5-a]azepin-9-yl)methyl acetate

There total 1 articles about phenyl(6,7,8,9-tetrahydro-5H-tetrazolo[1,5-a]azepin-9-yl)methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 54-95-5
pentetrazole

: 100-52-7
benzaldehyde

: 75-36-5
acetyl chloride

: 926290-85-9
phenyl(6,7,8,9-tetrahydro-5H-tetrazolo[1,5-a]azepin-9-yl)methyl acetate

Guidance literature:: pentetrazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

benzaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

acetyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1016/j.tetlet.2006.11.125