(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

Base Information

Chemical Name:(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}
CAS No.:134882-90-9
Molecular Formula:C₂₄H₂₀B*C₄₅H₄₇IrP₃
Molecular Weight:1192.24
Hs Code.:

(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Ir(C<sub>2</sub>H<sub>4</sub>)2<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup> = {(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Ir(C<sub>2</sub>H<sub>4</sub>)2}{B(C<sub>6</sub>H<sub>5</sub>)4}

Synonyms:(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

Suppliers and Price of (CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

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Chemical Property of (CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

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Technology Process of (CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

There total 2 articles about (CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 134882-83-0
[(1,1,1-tris(diphenylphosphinomethyl)ethane)Ir(C₂H₄)(H)2]BPh₄

: 74-85-1
ethene

: 134882-90-9
(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

Guidance literature:: In neat (no solvent); byproducts: C2H6; Ir-complex placing in glass apparatus, evacuation to <1E-4 Torr, immersing in oil bath maintained at90°C, reaction vessel backfilling with steady stream of C2H4 for 2 h; IR monitoring;
DOI:10.1021/ja00058a021

Reference yield:

: 134882-83-0
[(1,1,1-tris(diphenylphosphinomethyl)ethane)Ir(C₂H₄)(H)2]BPh₄

: 74-86-2,25067-58-7
acetylene

: 134882-90-9
(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

: 162761-41-3
Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₂H₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₂H₂)][B(C₆H₅)4]

: 162718-94-7
Ir(CH₃C(CH₂P(C₆H₅)2)3)(H)2(C₂H₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(CH₃C(CH₂P(C₆H₅)2)3)(H)2(C₂H₂)][B(C₆H₅)4]

: 162718-95-8
[(MeC(CH2PPh2)3)Ir((1-η(1):4-6-η(3))-hexatriene)]BPh4

Guidance literature:: In dichloromethane-d2; byproducts: [(MeC(CH2PPh2)3)Ir(η(4)-C6H6)]BPh4, ethene; NMR tube, -196°C; detd. by NMR spectroscopy;
DOI:10.1021/om00002a046

Reference yield: 95.0%

: 134882-90-9
(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

: 74-86-2,25067-58-7
acetylene

: 135006-00-7
(triphos)Ir(η4-benzene)(BPh4)

Guidance literature:: In tetrahydrofuran; dissolving Ir-complex under ethyne (1 atm) at room temperature, replacing ethyne with nitrogen after 1 h; addn. of ethanol, partial evapn. of solvent, filtn., washing (n-pentane), elem. anal.;
DOI:10.1021/om00017a067

upstream raw materials:

[(1,1,1-tris(diphenylphosphinomethyl)ethane)Ir(C₂H₄)(H)2]BPh₄

ethene

acetylene

Downstream raw materials:

(triphos)Ir(η4-benzene)(BPh4)

Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₂H₂)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₂H₂)][B(C₆H₅)4]

[(MeC(CH2PPh2)3)Ir((1-η(1):4-6-η(3))-hexatriene)]BPh4

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Encyclopedia

Technology Process of (CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

NAVIGATION

Encyclopedia

Technology Process of (CH3C(CH2P(C6H5)2)3)Ir(C2H4)2(1+)*B(C6H5)4(1-) = {(CH3C(CH2P(C6H5)2)3)Ir(C2H4)2}{B(C6H5)4}

(CH3C(CH2P(C6H5)2)3)Ir(C2H4)2(1+)*B(C6H5)4(1-) = {(CH3C(CH2P(C6H5)2)3)Ir(C2H4)2}{B(C6H5)4}

NAVIGATION

Technology Process of (CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}

(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2⁽¹⁺⁾*B(C₆H₅)4^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Ir(C₂H₄)2}{B(C₆H₅)4}