tert-butyl benzoyl(tert-butoxycarbonyl)carbamate

Base Information

Chemical Name:tert-butyl benzoyl(tert-butoxycarbonyl)carbamate
CAS No.:135364-97-5
Molecular Formula:C₁₇H₂₃NO₅
Molecular Weight:321.373
Hs Code.:

Synonyms:tert-butyl benzoyl(tert-butoxycarbonyl)carbamate

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Chemical Property of tert-butyl benzoyl(tert-butoxycarbonyl)carbamate

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Technology Process of tert-butyl benzoyl(tert-butoxycarbonyl)carbamate

There total 3 articles about tert-butyl benzoyl(tert-butoxycarbonyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 55-21-0,27208-38-4
benzamide

: 135364-97-5
tert-butyl benzoyl(tert-butoxycarbonyl)carbamate

Guidance literature:: With dmap; In acetonitrile; for 2h; Ambient temperature;
DOI:10.1021/jo00018a059

Reference yield:

: 98-88-4
benzoyl chloride

: 135364-97-5
tert-butyl benzoyl(tert-butoxycarbonyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide; triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2: dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; ammonium hydroxide; triethylamine; In dichloromethane;
DOI:10.1021/acs.joc.9b01699