8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY

Base Information

Chemical Name:8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY
CAS No.:1446281-33-9
Molecular Formula:C₂₇H₃₀BF₂N₃O
Molecular Weight:461.363
Hs Code.:

Synonyms:8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY

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Chemical Property of 8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY

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Technology Process of 8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY

There total 5 articles about 8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1218921-99-3
4,4-difluoro-8-(4-((succinimid-N-yl)oxycarbonyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene

: 2450-71-7
Propargylamine

: 1446281-33-9
8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/cs400332y

Reference yield: 72.0%

: 1033273-62-9
4,4-difluoro-8-(4-carboxyphenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-boron-3a,4a-diaza-s-indacene

: 2450-71-7
Propargylamine

: 1446281-33-9
8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/ic402798f

Reference yield: 56.0%

: 4-formyl-N-(prop-2-yn-1-yl)benzamide

: 517-22-6
2,4-dimethyl-3-ethyl-pyrrole

: 7637-07-2
boron trifluoride

: 1446281-33-9
8-(4-(N-(prop-2-yn-1-yl)benzamide))-2,8-diethyl-1,3,7,9-tetramethyl-BODIPY

Guidance literature:: 4-formyl-N-(prop-2-yn-1-yl)benzamide; 2,4-dimethyl-3-ethyl-pyrrole; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere; Darkness;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; at 20 ℃; for 1h;

boron trifluoride; With triethylamine; In diethyl ether; at 20 ℃;
DOI:10.1002/chem.201602886