C₁₅H₁₅⁽²⁾H₂NO₃

Base Information

Chemical Name:C₁₅H₁₅⁽²⁾H₂NO₃
CAS No.:1361110-39-5
Molecular Formula:C₁₅H₁₇NO₃
Molecular Weight:261.289
Hs Code.:

C<sub>15</sub>H<sub>15</sub><sup>(2)</sup>H<sub>2</sub>NO<sub>3</sub>

Synonyms:C₁₅H₁₅⁽²⁾H₂NO₃

Suppliers and Price of C₁₅H₁₅⁽²⁾H₂NO₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₅H₁₅⁽²⁾H₂NO₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₅H₁₅⁽²⁾H₂NO₃

There total 7 articles about C₁₅H₁₅⁽²⁾H₂NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1361111-15-0
C₁₄H₁₂⁽²⁾H₂N₂O

: 1361110-39-5
C₁₅H₁₅⁽²⁾H₂NO₃

Guidance literature:: methanol; C₁₄H₁₂⁽²⁾H₂N₂O; With sulfuric acid; at 0 ℃; Reflux;

With water; sodium hydrogencarbonate; In methanol;
DOI:10.1016/j.tetlet.2012.01.004

Reference yield:

: 98-01-1
furfural

: 1361110-39-5
C₁₅H₁₅⁽²⁾H₂NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / methanol / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 4 h / -78 °C / Inert atmosphere

2.3: Saturated solution

3.1: sulfuric acid / 0 °C / Reflux

With sulfuric acid; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004

Reference yield:

: 1361111-11-6
C₁₆H₁₃⁽²⁾H₂BrN₂

: 1361110-39-5
C₁₅H₁₅⁽²⁾H₂NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 0 °C / Reflux

2.1: palladium on activated charcoal; ammonium formate

3.1: potassium carbonate / methanol / 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: 4 h / -78 °C / Inert atmosphere

4.3: Saturated solution

5.1: sulfuric acid / 0 °C / Reflux

With sulfuric acid; palladium on activated charcoal; ammonium formate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004