4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene
CAS No.:1447031-68-6
Molecular Formula:C₂₃H₁₆BF₅N₂
Molecular Weight:426.196
Hs Code.:

Synonyms:4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene

Suppliers and Price of 4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene

There total 8 articles about 4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2089-33-0
4-methylacethophenone oxime

: 1447031-68-6
4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 6 steps

1.1: dimethyl sulfoxide / Alkaline conditions

2.1: pyridine / diethyl ether / 2.5 h

3.1: sodium hydrogencarbonate; sodium tetrahydroborate / methanol / 0.67 h

4.1: phosphorus pentoxide / dichloromethane / 16 h / 20 °C / Inert atmosphere

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

6.2: 1 h / 20 °C

With pyridine; sodium tetrahydroborate; phosphorus pentoxide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/ejoc.201300212

Reference yield:

: 109-63-7
boron trifluoride diethyl etherate

: C₂₃H₁₇F₃N₂

: 1447031-68-6
4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: C₂₃H₁₇F₃N₂; With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.166667h;

boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/ejoc.201300212

Reference yield:

: 1447004-23-0
1-[5-(4-methylphenyl)-1H-pyrrol-2-yl]-2,2,2-trifluoro-1-ethanol

: 1447031-68-6
4,4-difluoro-3-(4-methylphenyl)-5-phenyl-8-trifluoromethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphorus pentoxide / dichloromethane / 16 h / 20 °C / Inert atmosphere

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

3.2: 1 h / 20 °C

With phosphorus pentoxide; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1002/ejoc.201300212