triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside

Base Information

Chemical Name:triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside
CAS No.:140654-55-3
Molecular Formula:C₆₀H₅₆O₁₆S₂
Molecular Weight:1097.23
Hs Code.:

Synonyms:triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside

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Technology Process of triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside

There total 4 articles about triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 140654-54-2
triphenylmethyl 2,3,6-tri-O-benzoyl-4-O-trifluoromethanesulfonyl-1-thio-α-D-galactopyranoside

: 62860-10-0
2,3,4,6-tetra-O-acetyl-1-S-acetyl-1-thio-α-D-glucopyranoside

: 140654-55-3
triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside

Guidance literature:: With 1,4-dithio-erythritol; Cysteamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; for 2.5h; Ambient temperature;
DOI:10.1016/0008-6215(92)84093-8

Reference yield:

: 130718-48-8
triphenylmethyl 1-thio-α-D-galactopyranoside

: 140654-55-3
triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine / Ambient temperature

2: 2.26 g / pyridine / CH₂Cl₂ / 1.) 0 deg C, 30 min 2.) rt, 1 h

3: 75 percent / 1,4-dithioerythritol, cysteamine / hexamethylphosphoric acid triamide / 2.5 h / Ambient temperature

With pyridine; 1,4-dithio-erythritol; Cysteamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1016/0008-6215(92)84093-8

Reference yield:

: 98-88-4
benzoyl chloride

: 140654-55-3
triphenylmethyl 2,3,6-tri-O-benzoyl-4-S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1,4-dithio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine / Ambient temperature

2: 2.26 g / pyridine / CH₂Cl₂ / 1.) 0 deg C, 30 min 2.) rt, 1 h

3: 75 percent / 1,4-dithioerythritol, cysteamine / hexamethylphosphoric acid triamide / 2.5 h / Ambient temperature

With pyridine; 1,4-dithio-erythritol; Cysteamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1016/0008-6215(92)84093-8