(1S,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

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Chemical Name:(1S,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile
CAS No.:127253-91-2
Molecular Formula:C₂₄H₂₇N₃O₃Si
Molecular Weight:433.582
Hs Code.:

Synonyms:(1S,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

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Chemical Property of (1S,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

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Technology Process of (1S,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

There total 3 articles about (1S,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 941-69-5
N-phenyl-maleimide

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 101986-32-7
(-)-N-cyanomethyl-4-phenyl-1,3-oxazolidine

: 127196-23-0,127253-91-2,127253-92-3,127253-93-4
4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 4h;
DOI:10.1016/S0040-4039(01)93467-7

Reference yield:

: 941-69-5
N-phenyl-maleimide

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 101986-32-7
(-)-N-cyanomethyl-4-phenyl-1,3-oxazolidine

: 127196-23-0
(1R,3aR,6aS)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

: 127253-92-3
(1S,3aR,6aS)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

: 127253-93-4
(1R,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

: 127253-91-2
(1S,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 4h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(01)93467-7

Reference yield:

: 941-69-5
N-phenyl-maleimide

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 101986-32-7
(-)-N-cyanomethyl-4-phenyl-1,3-oxazolidine

: 127196-23-0
(1R,3aR,6aS)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

: 127253-91-2
(1S,3aS,6aR)-4,6-Dioxo-5-phenyl-2-((R)-1-phenyl-2-trimethylsilanyloxy-ethyl)-octahydro-pyrrolo[3,4-c]pyrrole-1-carbonitrile

Guidance literature:: With N-ethyl-N,N-diisopropylamine; Yield given. Yields of byproduct given; 1) CH₂Cl₂, -78 deg C, 4 h, 2) to r. t.;
DOI:10.1016/S0040-4020(01)90230-3