1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole

Base Information

Chemical Name:1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole
CAS No.:323178-41-2
Molecular Formula:C₃₄H₄₃NO₃S
Molecular Weight:545.786
Hs Code.:

Synonyms:1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole

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Chemical Property of 1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole

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Technology Process of 1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole

There total 8 articles about 1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 98-09-9
benzenesulfonyl chloride

: 323178-43-4
3-{(2E,6E)-3,7-Dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole

: 323178-41-2
1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole

Guidance literature:: With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate;
DOI:10.1016/S0040-4039(00)01528-8

Reference yield:

: 120-72-9
indole

: 323178-41-2
1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole

Guidance literature:: Multi-step reaction with 5 steps

1: EtMgBr / benzene / 20 °C

2: 72 percent / aq. KOH; Bu₄NHSO₄ / benzene / 20 °C

3: 83 percent / LDA; DMEU / tetrahydrofuran / -78 °C

4: 63 percent / EtNH₂; Li / methanol; diethyl ether / -78 °C

5: 95 percent / KOH; Bu₄NHSO₄

With 1,3-dimethyl-2-imidazolidinone; potassium hydroxide; ethylmagnesium bromide; tetra(n-butyl)ammonium hydrogensulfate; lithium; ethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; benzene;
DOI:10.1016/S0040-4039(00)01528-8

Reference yield:

: 64418-60-6
(E,E) O-acetyl 3,7-dimethyl-8-phenylsulfonyl-octa-2,6-diene-1-ol

: 323178-41-2
1-Benzenesulfonyl-3-{(2E,6E)-3,7-dimethyl-9-[(2R,3R)-3-methyl-3-(4-methyl-pent-3-enyl)-oxiranyl]-nona-2,6-dienyl}-1H-indole

Guidance literature:: Multi-step reaction with 7 steps

1: 80 percent / Na₂CO₃; MeOH

2: NBS; DMS / CH₂Cl₂ / -20 °C

3: EtMgBr / benzene / 20 °C

4: 72 percent / aq. KOH; Bu₄NHSO₄ / benzene / 20 °C

5: 83 percent / LDA; DMEU / tetrahydrofuran / -78 °C

6: 63 percent / EtNH₂; Li / methanol; diethyl ether / -78 °C

7: 95 percent / KOH; Bu₄NHSO₄

With 1,3-dimethyl-2-imidazolidinone; methanol; potassium hydroxide; N-Bromosuccinimide; 2,3-dimercapto-succinic acid; ethylmagnesium bromide; tetra(n-butyl)ammonium hydrogensulfate; lithium; sodium carbonate; ethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene;
DOI:10.1016/S0040-4039(00)01528-8