C₄₅H₅₃N₅O₁₆

Base Information

Chemical Name:C₄₅H₅₃N₅O₁₆
CAS No.:266676-43-1
Molecular Formula:C₄₅H₅₃N₅O₁₆
Molecular Weight:919.94
Hs Code.:

C<sub>45</sub>H<sub>53</sub>N<sub>5</sub>O<sub>16</sub>

Synonyms:C₄₅H₅₃N₅O₁₆

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Chemical Property of C₄₅H₅₃N₅O₁₆

Chemical Property:

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Technology Process of C₄₅H₅₃N₅O₁₆

There total 14 articles about C₄₅H₅₃N₅O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 30516-87-1,399024-19-2
3'-azido-2',3'-deoxythymidine

: 266676-42-0
C₃₅H₄₂O₁₃

: 266676-43-1
C₄₅H₅₃N₅O₁₆

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In toluene;
DOI:10.1016/S0960-894X(00)00031-7

Reference yield:

: 11034-45-0
1β,2α,9α,10β-tetrahydroxy-5α-cinnamoyloxytaxa-4(20),11-dien-13-one

: 266676-43-1
C₄₅H₅₃N₅O₁₆

Guidance literature:: Multi-step reaction with 13 steps

1: 73 percent / CuSO₄

2: 92 percent / pyridine / CH₂Cl₂ / 0 °C

3: 65 percent / aq. H₂NOH*HCl; NaOAc / ethanol / Heating

4: 86 percent / aq. OsO₄; NMO / tetrahydrofuran / 20 °C

5: 95 percent / imidazole / dimethylformamide / 20 °C

6: 81 percent / pyridine

7: TBAF / tetrahydrofuran

8: Bu₄N⁺AcO^- / butan-2-one / Heating

9: 71 percent / aq. AcOH / tetrahydrofuran / 40 °C

10: 76 percent / DMAP / 0 - 20 °C

11: 84 percent / tetrahydrofuran / -78 °C

12: 69 percent / DMAP / dimethylformamide / 48 h / 85 °C

13: 85 percent / DCC; DMAP / toluene

With pyridine; 1H-imidazole; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium acetate; tetrabutylammonium acetate; copper(II) sulfate; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; butanone; 1: ketalization / 2: cyclocondensation / 3: Hydrolysis / 4: dihydroxylation / 5: silylation / 6: mesylation / 7: desilylation / 8: Cyclization / 9: deketalization / 10: Acetylation / 11: Addition / 12: Addition / 13: Esterification;
DOI:10.1016/S0960-894X(00)00031-7

Reference yield:

: 13452-36-3
2,9,10-triacetyl-5-O-cinnamoyltaxicin-I

: 266676-43-1
C₄₅H₅₃N₅O₁₆

Guidance literature:: Multi-step reaction with 14 steps

1: 86 percent / NaOCH₃ / methanol; CH₂Cl₂ / 0 °C

2: 73 percent / CuSO₄

3: 92 percent / pyridine / CH₂Cl₂ / 0 °C

4: 65 percent / aq. H₂NOH*HCl; NaOAc / ethanol / Heating

5: 86 percent / aq. OsO₄; NMO / tetrahydrofuran / 20 °C

6: 95 percent / imidazole / dimethylformamide / 20 °C

7: 81 percent / pyridine

8: TBAF / tetrahydrofuran

9: Bu₄N⁺AcO^- / butan-2-one / Heating

10: 71 percent / aq. AcOH / tetrahydrofuran / 40 °C

11: 76 percent / DMAP / 0 - 20 °C

12: 84 percent / tetrahydrofuran / -78 °C

13: 69 percent / DMAP / dimethylformamide / 48 h / 85 °C

14: 85 percent / DCC; DMAP / toluene

With pyridine; 1H-imidazole; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium methylate; sodium acetate; tetrabutylammonium acetate; copper(II) sulfate; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; butanone; 1: Deacetylation / 2: ketalization / 3: cyclocondensation / 4: Hydrolysis / 5: dihydroxylation / 6: silylation / 7: mesylation / 8: desilylation / 9: Cyclization / 10: deketalization / 11: Acetylation / 12: Addition / 13: Addition / 14: Esterification;
DOI:10.1016/S0960-894X(00)00031-7