2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Base Information

Chemical Name:2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol
CAS No.:1253119-89-9
Molecular Formula:C₃₂H₂₅N₅O₇
Molecular Weight:591.58
Hs Code.:

Synonyms:2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

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Chemical Property of 2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

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Technology Process of 2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

There total 13 articles about 2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1253119-88-8
2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole

: 1253119-89-9
2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Guidance literature:: 2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole; With boron tribromide; In dichloromethane; at -78 - 0 ℃;

With methanol; In dichloromethane;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1253119-89-9
2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / dimethyl sulfoxide / 12 h / 130 °C

2: hydrogenchloride / water / 12 h / 110 °C

3: hydrazine hydrate / ethanol / 24 h / Reflux

4: tetrahydrofuran / 12 h / 20 °C

5: trichlorophosphate / 12 h / 90 °C

6: boron tribromide / dichloromethane / -78 - 0 °C

With hydrogenchloride; boron tribromide; potassium carbonate; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 27237-21-4
3-(4-nitrophenoxy)benzoic acid

: 1253119-89-9
2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / water / 12 h / 110 °C

2: hydrazine hydrate / ethanol / 24 h / Reflux

3: tetrahydrofuran / 12 h / 20 °C

4: trichlorophosphate / 12 h / 90 °C

5: boron tribromide / dichloromethane / -78 - 0 °C

With hydrogenchloride; boron tribromide; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; water;