2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole

Base Information

Chemical Name:2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole
CAS No.:1253119-88-8
Molecular Formula:C₄₄H₄₉N₅O₇
Molecular Weight:759.902
Hs Code.:

Synonyms:2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole

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Chemical Property of 2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole

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Technology Process of 2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole

There total 13 articles about 2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1253119-87-7
N'-1-(4-t-butylbenzoyl)-2,5-bis(hexyloxy)-N'-4-(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide

: 1253119-88-8
2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole

Guidance literature:: With trichlorophosphate; at 90 ℃; for 12h;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1253119-88-8
2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / dimethyl sulfoxide / 12 h / 130 °C

2: hydrogenchloride / water / 12 h / 110 °C

3: hydrazine hydrate / ethanol / 24 h / Reflux

4: tetrahydrofuran / 12 h / 20 °C

5: trichlorophosphate / 12 h / 90 °C

With hydrogenchloride; potassium carbonate; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide;

Reference yield:

: 27237-21-4
3-(4-nitrophenoxy)benzoic acid

: 1253119-88-8
2-(2,5-bis(hexyloxy)-4-(5-(3-(4-nitrophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)phenyl)-5-(4-t-butylphenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / water / 12 h / 110 °C

2: hydrazine hydrate / ethanol / 24 h / Reflux

3: tetrahydrofuran / 12 h / 20 °C

4: trichlorophosphate / 12 h / 90 °C

With hydrogenchloride; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; ethanol; water;