2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene

Base Information

Chemical Name:2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene
CAS No.:129363-21-9
Molecular Formula:C₂₅H₁₈Cl₂N₂O
Molecular Weight:433.337
Hs Code.:

Synonyms:2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene

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Chemical Property of 2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene

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Technology Process of 2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene

There total 2 articles about 2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129337-86-6
2-chloro-5,6,7,8-tetrahydroquinolin-8-one

: 130861-82-4
7-benzylidene-2-chloro-5,6,7,8-tetrahydro-8-quinolone

: 129363-21-9
2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene

Guidance literature:: With boron trifluoride diethyl etherate;
DOI:10.1021/jo00303a006

Reference yield:

: 100-52-7
benzaldehyde

: 129363-21-9
2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / KOH / methanol; H₂O / Ambient temperature

2: boron trifluoride etherate / 0.5 h / 110 °C

With potassium hydroxide; boron trifluoride diethyl etherate; In methanol; water;
DOI:10.1021/ja00001a027

Reference yield:

: 129363-21-9
2,12-Dichloro-7-phenyl-5,7,8,9-tetrahydro-6H-14-oxa-1,13-diaza-dibenzo[a,j]anthracene

: 129337-88-8
methyl 2,12-dichloro-7-phenyl-1,13-diazadibenzanthracene-14-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: 41 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / various solvent(s) / 20 h / Heating

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In various solvent(s);
DOI:10.1021/ja00001a027