(S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal

Base Information

Chemical Name:(S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal
CAS No.:1236479-43-8
Molecular Formula:C₁₈H₂₁NO₄
Molecular Weight:315.369
Hs Code.:

Synonyms:(S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal

Suppliers and Price of (S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal

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Technology Process of (S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal

There total 1 articles about (S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1236479-42-7
(S)-4-benzyl-3-((S)-6-hydroxy-2-methyl-4-methylenehexanoyl)oxazolidin-2-one

: 1236479-43-8
(S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal

Guidance literature:: With Dess-Martin periodane; In dichloromethane; water; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.012

Reference yield:

: 1236479-43-8
(S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal

: 2234-82-4
1-propylmagnesium chloride

: (S)-4-benzyl-3-((2S,6R)-6-hydroxy-2-methyl-4-methylenenonanoyl)oxazolidin-2-one

: (S)-4-benzyl-3-((2S,6S)-6-hydroxy-2-methyl-4-methylenenonanoyl)oxazolidin-2-one

Guidance literature:: (S)-6-((S)-4-benzyl-2-oxooxazolidin-3-yl)-5-methyl-3-methylene-6-oxohexanal; 1-propylmagnesium chloride; In diethyl ether; at -78 ℃; Inert atmosphere;

With ammonium chloride; In diethyl ether; water; at 20 ℃; for 0.5h; optical yield given as %de; diastereoselective reaction; Saturated solution;
DOI:10.1016/j.tet.2010.05.012