(S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol

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Chemical Name:(S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol
CAS No.:1203466-56-1
Molecular Formula:C₁₆H₁₆O₅S₂
Molecular Weight:352.432
Hs Code.:

Synonyms:(S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol

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Chemical Property of (S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol

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Technology Process of (S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol

There total 1 articles about (S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1222468-58-7
(S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propionaldehyde

: 1203466-56-1
(S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.333333h; enantioselective reaction;
DOI:10.1016/j.tetlet.2010.01.102

Reference yield: 97.0%

: 1203466-56-1
(S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1222468-85-0
tert-butyl-dimethyl-[3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propoxy]-silane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2010.01.102

Reference yield: 90.0%

: 1203466-56-1
(S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol

: 1222468-83-8
(S)-3-(2-fluoro-1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-3-phenyl-propan-1-ol

Guidance literature:: (S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propan-1-ol; With potassium tert-butylate; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

With Selectfluor; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; enantioselective reaction;
DOI:10.1016/j.tetlet.2010.01.102