1,3-di-[4-amino-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercapto propane

Base Information

Chemical Name:1,3-di-[4-amino-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercapto propane
CAS No.:936259-74-4
Molecular Formula:C₁₉H₂₀N₈O₂S₂
Molecular Weight:456.552
Hs Code.:

Synonyms:1,3-di-[4-amino-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercapto propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-di-[4-amino-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercapto propane

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Technology Process of 1,3-di-[4-amino-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercapto propane

There total 2 articles about 1,3-di-[4-amino-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercapto propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 22706-15-6
2-(4-amino-5-mercapto-[1,2,4]triazol-3-yl)phenol

: 109-64-8
1,3-dibromo-propane

: 936259-74-4
1,3-di-[4-amino-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercapto propane

Guidance literature:: With potassium hydroxide; In methanol; water; at 80 ℃; for 8h;
DOI:10.1139/V06-181

Reference yield:

: 936-02-7
2-Hydroxybenzoylhydrazine

: 936259-74-4
1,3-di-[4-amino-5(2'-hydroxyphenyl)-1,2,4-triazol-3-yl]mercapto propane

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / methanol / 0 - 5 °C

1.2: 80 percent / hydrazine hydrate / 4 h / 90 °C

2.1: 65 percent / potassium hydroxide / methanol; H₂O / 8 h / 80 °C

With potassium hydroxide; In methanol; water;
DOI:10.1139/V06-181