tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate

Base Information

Chemical Name:tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate
CAS No.:949109-36-8
Molecular Formula:C₁₇H₂₅N₃O₆S
Molecular Weight:399.468
Hs Code.:

Synonyms:tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate

Suppliers and Price of tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(S)-tert-Butyl3-methyl-4-((2-nitrophenyl)sulfonyl)-1,4-diazepane-1-carboxylate 97%
25g
$ 223.00

Chemenu
(S)-tert-Butyl3-methyl-4-((2-nitrophenyl)sulfonyl)-1,4-diazepane-1-carboxylate 97%
25g
$ 210.00

Chemenu
(S)-tert-Butyl3-methyl-4-((2-nitrophenyl)sulfonyl)-1,4-diazepane-1-carboxylate 97%
10g
$ 122.00

Alichem
(S)-tert-Butyl3-methyl-4-((2-nitrophenyl)sulfonyl)-1,4-diazepane-1-carboxylate
25g
$ 227.25

Total 6 raw suppliers

Chemical Property of tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

(S)-tert-Butyl3-methyl-4-((2-nitrophenyl)sulfonyl)-1,4-diazepane-1-carboxylate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate

There total 8 articles about tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.2%

: 24424-99-5
di-tert-butyl dicarbonate

: (S)-2-methyl-1-(2-nitrophenylsulfonyl)-1,4-diazepane hydrochloride

: 949109-36-8
tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate

Guidance literature:: With potassium carbonate; In ethanol; water; at 5 ℃; for 5h; Large scale;

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1360538-88-0
(S)-2-methyl-1-[(2-nitrophenyl)sulfonyl]-1,4-diazepane hydrochloride

: 949109-36-8
tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate

Guidance literature:: With potassium carbonate; In ethanol; water; Inert atmosphere; Large scale;
DOI:10.1055/s-0032-1316771

Reference yield: 74.5%

: 949109-35-7
(S)-tert-butyl 3-hydroxypropyl(2-(2-nitrophenylsulfonylamide)propyl)carbamate

: 949109-36-8
tert-butyl (S)-3-methyl-4-[(2-nitrophenyl)sulfonyl]-1,4-diazepane-1-carboxylate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 5 - 20 ℃; for 9h; Inert atmosphere; Large scale;