(S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide

Base Information

Chemical Name:(S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide
CAS No.:1360538-87-9
Molecular Formula:C₁₂H₁₉N₃O₅S
Molecular Weight:317.366
Hs Code.:

Synonyms:(S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide

Suppliers and Price of (S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide

Chemical Property:

Purity/Quality:: 95%-98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide

There total 4 articles about (S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 156-87-6
propan-1-ol-3-amine

: (S)-N-(1-methanesulfonyloxypropan-2-yl)-2-nitrobenzenesulfonamide

: 1360538-87-9
(S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide

Guidance literature:: In acetonitrile; at 0 - 20 ℃; Inert atmosphere; Large scale;
DOI:10.1055/s-0032-1316771

Reference yield:

: 1411975-57-9
(R)-N-(2-hydroxy-1-methylethyl)-2-nitrobenzenesulfonamide

: 1360538-87-9
(S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine / dichloromethane / 0 - 20 °C / Inert atmosphere; Large scale

2: acetonitrile / 0 - 20 °C / Inert atmosphere; Large scale

With 4-methyl-morpholine; In dichloromethane; acetonitrile;
DOI:10.1055/s-0032-1316771

Reference yield:

: N-[(1S)-2-hydroxy-1-methylethyl]-2-nitrobenzenesulfonamide

: 1360538-87-9
(S)-N-{1-[(3-hydroxypropyl)amino]propan-2-yl}-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine / dichloromethane / 20 h / -5 - 20 °C / Large scale

2: potassium carbonate / acetonitrile / 16 h / 10 - 20 °C / Large scale

With 4-methyl-morpholine; potassium carbonate; In dichloromethane; acetonitrile;