methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate

Base Information

Chemical Name:methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate
CAS No.:415949-82-5
Molecular Formula:C₂₄H₂₃BrO₄
Molecular Weight:455.348
Hs Code.:

Synonyms:methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate

Suppliers and Price of methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate

There total 2 articles about methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 399-55-3
2-fluoro-1-methoxy-4-methylbenzene

: 415949-73-4
methyl (2-benzyloxy-3-bromophenyl)acetate

: 415949-82-5
methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate

Guidance literature:: 2-fluoro-1-methoxy-4-methylbenzene; With chromium⁽⁰⁾ hexacarbonyl; In tetrahydrofuran; dibutyl ether; at 125 ℃; for 72h; exclusion of daylight;

methyl (2-benzyloxy-3-bromophenyl)acetate; With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.333333h;

In tetrahydrofuran; diethyl ether; for 1h; Irradiation;
DOI:10.1002/1099-0690(20021)2002:2<369::AID-EJOC369>3.0.CO;2-7

Reference yield:

: 2-methoxy-5-methyldiazonium tetrafluoroborate

: 415949-82-5
methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 73 percent / BF₃*Et₂O / 0 °C / Irradiation

2.1: Cr(CO)6 / tetrahydrofuran; dibutyl ether / 72 h / 125 °C / exclusion of daylight

2.2: KOH / dimethylsulfoxide / 0.33 h / 20 °C

2.3: tetrahydrofuran; diethyl ether / 1 h / Irradiation

With boron trifluoride diethyl etherate; chromium⁽⁰⁾ hexacarbonyl; In tetrahydrofuran; dibutyl ether;
DOI:10.1002/1099-0690(20021)2002:2<369::AID-EJOC369>3.0.CO;2-7

Reference yield: 59.0%

: 415949-82-5
methyl 2-[2-benzyloxy-3-bromophenyl]-2-(2-methoxy-5-methylphenyl)acetate

: 415949-83-6
methyl 2-(2-hydroxyphenyl)-2-(2-methoxy-5-methylphenyl)acetate

Guidance literature:: With hydrogen; trifluoroacetic acid; palladium dihydroxide; In tetrahydrofuran; ethanol; at 20 ℃; for 12h;
DOI:10.1002/1099-0690(20021)2002:2<369::AID-EJOC369>3.0.CO;2-7