Technology Process of C30H22N2
There total 1 articles about C30H22N2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
1,2-dimethoxyethane; water; toluene;
for 15h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate;
In
toluene;
for 8h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 8 h / Inert atmosphere; Reflux
2.1: palladium diacetate; tricyclohexylphosphine tetrafluoroborate; potassium carbonate / N,N-dimethyl acetamide / 15 h / 130 °C / Inert atmosphere
3.1: tris-(dibenzylideneacetone)dipalladium(0); tri tert-butylphosphoniumtetrafluoroborate / 5,5-dimethyl-1,3-cyclohexadiene / Inert atmosphere; Reflux
3.2: 2 h
With
tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tricyclohexylphosphine tetrafluoroborate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate;
In
5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl acetamide; toluene;