hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium

Base Information

Chemical Name:hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium
CAS No.:71195-76-1
Molecular Formula:C₈H₉O₅S*Na
Molecular Weight:240.212
Hs Code.:

Synonyms:hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium

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Chemical Property of hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium

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Technology Process of hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium

There total 1 articles about hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 71195-76-1
hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium

Guidance literature:: With sodium disulfite;

Reference yield: 67.0%

: 71195-76-1
hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium

: 38359-80-7
ethyl <4,5-diamino-6-<(diphenylmethyl)amino>pyridin-2-yl>carbamate dihydrochloride

: 109182-54-9
ethyl 2-(4-methoxyphenyl)-4-<(diphenylmethyl)amino>-1H-imidazo<4,5-c>pyridin-6-ylcarbamate

Guidance literature:: With sodium ethanolate; In ethanol; for 168h; Ambient temperature;
DOI:10.1021/jm00393a011

Reference yield:

: 71195-76-1
hydroxy-(4-methoxy-phenyl)-methanesulfonic acid ; anisaldehyde sulfite sodium

: 109182-58-3
ethyl 4-amino-2-(4-methoxyphenyl)-1H-imidazo<4,5-c>pyridin-6-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / EtONa / ethanol / 168 h / Ambient temperature

2: 40.5 percent / conc. HCl / 164 h / 25 °C

With hydrogenchloride; sodium ethanolate; In ethanol;
DOI:10.1021/jm00393a011