N,N',N-tris(p-anisyl)azacolix[3](2,6)(4-pyrrolidinopyridine) hydrogen bromide

Base Information

Chemical Name:N,N',N-tris(p-anisyl)azacolix[3](2,6)(4-pyrrolidinopyridine) hydrogen bromide
CAS No.:1408315-40-1
Molecular Formula:BrH*C₄₈H₅₁N₉O₃
Molecular Weight:882.903
Hs Code.:

Synonyms:N,N',N-tris(p-anisyl)azacolix[3](2,6)(4-pyrrolidinopyridine) hydrogen bromide

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Chemical Property of N,N',N-tris(p-anisyl)azacolix[3](2,6)(4-pyrrolidinopyridine) hydrogen bromide

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Technology Process of N,N',N-tris(p-anisyl)azacolix[3](2,6)(4-pyrrolidinopyridine) hydrogen bromide

There total 2 articles about N,N',N-tris(p-anisyl)azacolix[3](2,6)(4-pyrrolidinopyridine) hydrogen bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1253182-42-1
2,6-dibromo-4-(pyrrolidin-1-yl)pyridine

: 1408315-40-1
N,N',N-tris(p-anisyl)azacolix[3](2,6)(4-pyrrolidinopyridine) hydrogen bromide

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / toluene / 18 h / 100 °C / Inert atmosphere

2: copper(I) bromide; potassium carbonate / nitrobenzene / 3 h / 190 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; copper(I) bromide; sodium t-butanolate; In nitrobenzene; toluene;
DOI:10.1021/jo3017428

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1408315-40-1
N,N',N-tris(p-anisyl)azacolix[3](2,6)(4-pyrrolidinopyridine) hydrogen bromide

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / toluene / 18 h / 100 °C / Inert atmosphere

2: copper(I) bromide; potassium carbonate / nitrobenzene / 3 h / 190 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; copper(I) bromide; sodium t-butanolate; In nitrobenzene; toluene;
DOI:10.1021/jo3017428