(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate

Base Information

Chemical Name:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate
CAS No.:75468-42-7
Molecular Formula:C₃₀H₃₅O₂P
Molecular Weight:458.58
Hs Code.:

Synonyms:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate

Suppliers and Price of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate

Chemical Property:

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Technology Process of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate

There total 4 articles about (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 16832-20-5,32815-12-6,55284-67-8
(1R,2S,5R)-menthol bromoacetate

: 603-35-0
triphenylphosphine

: 75468-42-7
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate

Guidance literature:: (1R,2S,5R)-menthol bromoacetate; triphenylphosphine; In tetrahydrofuran; for 2h; Inert atmosphere;

With sodium hydroxide; In tetrahydrofuran; toluene; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.09.010

Reference yield:

: 2216-51-5
(-)-menthol

: 75468-42-7
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(triphenylphosphoranylidene)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2: tetrahydrofuran / 2.5 h / Inert atmosphere; Reflux

3: sodium hydroxide / water; toluene / 3.08 h / Inert atmosphere

With triethylamine; sodium hydroxide; In tetrahydrofuran; water; toluene;
DOI:10.1039/c3ob27111k