,S^)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

Base Information

Chemical Name:*,S^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine
CAS No.:147165-89-7
Molecular Formula:C₁₆H₂₃NO₂
Molecular Weight:261.364
Hs Code.:

<S-(R<sup>*</sup>,S<sup>*</sup>)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

Synonyms:*,S^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of *,S^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

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Technology Process of *,S^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

There total 3 articles about *,S^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 147165-82-0
*,S^*)>-N-hydroxy-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

: 147165-89-7
*,S^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

Guidance literature:: With copper(II) sulfate; acetic acid; zinc; In water; at 70 ℃; for 1h;

Reference yield:

: 100777-91-1
(2S)-2,3-O-isopropylideneglyceraldehyde N-benzylimine

: 1730-25-2
allylmagnesium bromide

: 147165-86-4
*,R^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

: 147165-89-7
*,S^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

Guidance literature:: In diethyl ether; at -20 ℃; for 12h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/c1ob06216f

Reference yield:

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 147165-89-7
*,S^*)>-2,2-dimethyl-N-(phenylmethyl)-α-(2-propenyl)-1,3-dioxolane-4-methanamine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / -30 °C

2: 75 percent / Zn, CuSO₄, glacial acetic acid / H₂O / 1 h / 70 °C

With copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; water;