(2R,5S)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1] octane-2-carboxylic acid cyclohexylamine salt

Base Information

Chemical Name:(2R,5S)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1] octane-2-carboxylic acid cyclohexylamine salt
CAS No.:1383814-71-8
Molecular Formula:C₆H₁₃N*C₁₄H₁₆N₂O₄
Molecular Weight:375.468
Hs Code.:

Synonyms:(2R,5S)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1] octane-2-carboxylic acid cyclohexylamine salt

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Chemical Property of (2R,5S)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1] octane-2-carboxylic acid cyclohexylamine salt

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Technology Process of (2R,5S)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1] octane-2-carboxylic acid cyclohexylamine salt

There total 2 articles about (2R,5S)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1] octane-2-carboxylic acid cyclohexylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1383814-69-4
(2R,5S)-tert-butyl 6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1]octane-2-carboxylate

: 108-91-8,157973-60-9
cyclohexylamine

: 1383814-71-8
(2R,5S)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1] octane-2-carboxylic acid cyclohexylamine salt

Guidance literature:: (2R,5S)-tert-butyl 6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1]octane-2-carboxylate; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;

cyclohexylamine; In diethyl ether; ethyl acetate; at 0 - 20 ℃; for 1h;

Reference yield:

: C₁₇H₂₆N₂O₃

: 1383814-71-8
(2R,5S)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1] octane-2-carboxylic acid cyclohexylamine salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / acetonitrile / 0.25 h / 0 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;