Technology Process of 3-(3-chloropropylsulfonyl)aniline
There total 4 articles about 3-(3-chloropropylsulfonyl)aniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 20 ℃;
for 16h;
under 1125.11 - 1500.15 Torr;
DOI:10.1002/cmdc.201200264
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine; tetrachloromethane / chloroform / 48 h / 20 °C
2: potassium nitrate; sulfuric acid / 6 h / 70 °C
3: palladium on activated charcoal; hydrogen / methanol / 16 h / 20 °C / 1125.11 - 1500.15 Torr
With
tetrachloromethane; sulfuric acid; palladium on activated charcoal; hydrogen; potassium nitrate; triphenylphosphine;
In
methanol; chloroform;
1: |Appel Halogenation;
DOI:10.1002/cmdc.201200264
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrabutylammomium bromide; sodium iodide / water; chloroform / 16 h / Reflux
2: triphenylphosphine; tetrachloromethane / chloroform / 48 h / 20 °C
3: potassium nitrate; sulfuric acid / 6 h / 70 °C
4: palladium on activated charcoal; hydrogen / methanol / 16 h / 20 °C / 1125.11 - 1500.15 Torr
With
tetrachloromethane; sulfuric acid; palladium on activated charcoal; tetrabutylammomium bromide; hydrogen; potassium nitrate; triphenylphosphine; sodium iodide;
In
methanol; chloroform; water;
2: |Appel Halogenation;
DOI:10.1002/cmdc.201200264
