[1-⁽²⁾H₁]-pentanal

Base Information

Chemical Name:[1-⁽²⁾H₁]-pentanal
CAS No.:35667-35-7
Molecular Formula:C₅H₁₀O
Molecular Weight:87.1259
Hs Code.:

[1-<sup>(2)</sup>H<sub>1</sub>]-pentanal

Synonyms:[1-⁽²⁾H₁]-pentanal

Suppliers and Price of [1-⁽²⁾H₁]-pentanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1-⁽²⁾H₁]-pentanal

Chemical Property:

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Technology Process of [1-⁽²⁾H₁]-pentanal

There total 2 articles about [1-⁽²⁾H₁]-pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78362-94-4
{PPN}{HCr(CO)5}

: 1455-13-6
deuteromethanol

: 638-29-9
n-valeryl chloride

: 65650-76-2
bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}

: 35667-35-7
[1-⁽²⁾H₁]-pentanal

Guidance literature:: In tetrahydrofuran; 1:1 molar ratio, THF, 25°C;; detected by NMR and IR spectra; and GC analysis,;

Reference yield: 61.0%

: 109-72-8,29786-93-4
n-butyllithium

: 2914-27-4
d1-N,N-dimethylformamide

: 35667-35-7
[1-⁽²⁾H₁]-pentanal

Guidance literature:: In tetrahydrofuran; diethyl ether; hexane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201202080

Reference yield:

: 35667-35-7
[1-⁽²⁾H₁]-pentanal

: 1393604-75-5
(4R)-1-(p-tolylsulfonyloxy)-[4-⁽²⁾H₁]-oct-2-yne

Guidance literature:: Multi-step reaction with 5 steps

1.1: B-isopinocampheyl-9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

2.1: potassium hydroxide / diethyl ether / 2 h / -50 - 0 °C

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; methyllithium / diethyl ether / 0.75 h / 0 °C / Inert atmosphere

3.2: 50.5 h / 0 - 45 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / methanol / 4 h / 0 - 20 °C

5.1: potassium hydroxide / diethyl ether / 2 h / -50 - 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; B-isopinocampheyl-9-borabicyclo[3.3.1]nonane; methyllithium; toluene-4-sulfonic acid; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/anie.201202080