1-acetoxyethyl phenyl sulfide

Base Information

• Chemical Name: 1-acetoxyethyl phenyl sulfide
• CAS No.: 91922-48-4
• Molecular Formula: C₁₀H₁₂O₂S
• Molecular Weight: 196.27
• Mol file: 91922-48-4.mol

Synonyms:1-acetoxyethyl phenyl sulfide

Chemical Property of 1-acetoxyethyl phenyl sulfide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-acetoxyethyl phenyl sulfide

There total 5 articles about 1-acetoxyethyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

vinyl acetate (108-05-4,9003-20-7) + thiophenol (108-98-5) → 1-acetoxyethyl phenyl sulfide (91922-48-4)

Guidance literature:

With 1-pentyl-3-methylimidazolium bromide; at 20 ℃; for 0.75h; regioselective reaction;

Reference yield: 50.0%

Ethyl phenyl sulfide (622-38-8) + acetic acid (64-19-7,77671-22-8) → 1-acetoxyethyl phenyl sulfide (91922-48-4)

Guidance literature:

With tetrabutylammonium tetrafluoroborate; In methanol; acetonitrile; at 20 ℃; for 6h; Inert atmosphere; Electrochemical reaction;

DOI:10.1021/jacs.1c00288

Reference yield: 47.0%

1-chloroethyl phenyl sulfide (13557-24-9) + sodium acetate (127-09-3) → 1-acetoxyethyl phenyl sulfide (91922-48-4)

Guidance literature:

In N,N-dimethyl-formamide; 1.) 50 deg C, 1 h, 2.) RT, 18 h;

upstream raw materials:

1-chloroethyl phenyl sulfide

sodium acetate

Ethyl phenyl sulfide

acetic acid

Downstream raw materials:

1-acetoxyethyl phenyl sulfoxide