(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

Base Information

• Chemical Name: (C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄
• CAS No.: 32610-60-9
• Molecular Formula: BF₄*C₂₇H₂₆FeO₂P
• Molecular Weight: 556.128

Synonyms:(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

Chemical Property of (C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

There total 2 articles about (C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(OCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

acetyl carbonyl cyclopentadienyl triphenylphosphine iron + trimethoxonium tetrafluoroborate (420-37-1) → (C5H5)Fe(C(OCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(OCH3)CH3)(CO)(P(C6H5)3)]BF4 (32610-60-9)

Guidance literature:

In not given; (N2); stirring (room temp., 8 h); filtration via cannula, concn. (vac.), dissoln. (min. amt. CH2Cl2), cannulation into Et2O, pptn. upon cooling to 0°C, removal of solvent via cannula, washing (Et2O), drying (vac.), recrystn. (CH2Cl2/Et2O);

DOI:10.1039/a800927i

Reference yield: 70.0%

{Cp(CO)(Ph3P)FeCCH2}BF4 → (C5H5)Fe(C(OCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(OCH3)CH3)(CO)(P(C6H5)3)]BF4 (32610-60-9)

Guidance literature:

With methanol; In methanol; The complex was dissolved in MeOH, 0.25 h (N2 atm.);; evapd., recrystd. from CH2Cl2-Et2O;;

Reference yield: 96.0%

(C5H5)Fe(C(OCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(OCH3)CH3)(CO)(P(C6H5)3)]BF4 (32610-60-9) + methylamine (74-89-5) → (C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)]BF4 (80662-48-2)

Guidance literature:

In tetrahydrofuran; (N2); concn. (vac.), dissoln. (min. amt. CH2Cl2), pptn. upon cannulation into Et2O at 0°C, removal of solvent, washing (Et2O), drying (vac.);

DOI:10.1039/a800927i

upstream raw materials:

trimethoxonium tetrafluoroborate

Downstream raw materials:

(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)⁽¹⁺⁾*BF₄^(1-) = [(C₅H₅)Fe(C(NHCH₃)CH₃)(CO)(P(C₆H₅)3)]BF₄

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