Technology Process of CH3COC6H4CO2C6H4CO2C6H5(CO2C6H4)2
There total 4 articles about CH3COC6H4CO2C6H4CO2C6H5(CO2C6H4)2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 89 percent / pyridine / 2 h / 20 °C
2: 77 percent / phenyltrimethylammonium tribromide / tetrahydrofuran / 6 h / 20 °C
3: 73 percent / acetonitrile / 48 h / 20 °C
4: NaH / tetrahydrofuran / Heating
With
pyridine; phenyltrimethylammonium tribromide; sodium hydride;
In
tetrahydrofuran; acetonitrile;
1: Acylation / 2: Bromination / 3: Substitution / 4: Rearrangement;
DOI:10.1021/jo990735q
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 77 percent / phenyltrimethylammonium tribromide / tetrahydrofuran / 6 h / 20 °C
2: 73 percent / acetonitrile / 48 h / 20 °C
3: NaH / tetrahydrofuran / Heating
With
phenyltrimethylammonium tribromide; sodium hydride;
In
tetrahydrofuran; acetonitrile;
1: Bromination / 2: Substitution / 3: Rearrangement;
DOI:10.1021/jo990735q
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 89 percent / pyridine / 2 h / 20 °C
2: 77 percent / phenyltrimethylammonium tribromide / tetrahydrofuran / 6 h / 20 °C
3: 73 percent / acetonitrile / 48 h / 20 °C
4: NaH / tetrahydrofuran / Heating
With
pyridine; phenyltrimethylammonium tribromide; sodium hydride;
In
tetrahydrofuran; acetonitrile;
1: Acylation / 2: Bromination / 3: Substitution / 4: Rearrangement;
DOI:10.1021/jo990735q
