tris(4-chlorophenyl)bismuth difluoride

Base Information

Chemical Name:tris(4-chlorophenyl)bismuth difluoride
CAS No.:121899-91-0
Molecular Formula:C₁₈H₁₂BiCl₃F₂
Molecular Weight:581.629
Hs Code.:

Synonyms:tris(4-chlorophenyl)bismuth difluoride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(4-chlorophenyl)bismuth difluoride

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Technology Process of tris(4-chlorophenyl)bismuth difluoride

There total 2 articles about tris(4-chlorophenyl)bismuth difluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: xenon fluoride

: 5575-51-9
tris(4-chlorophenyl)bismuthane

: 121899-91-0
tris(4-chlorophenyl)bismuth difluoride

Guidance literature:: In dichloromethane; Ar-atmosphere; 0°C;
DOI:10.1021/om990597v

Reference yield: 90.0%

: 77760-10-2
tris(4-chlorophenyl)bismuth dichloride

: 11113-87-4
silver fluoride

: 121899-91-0
tris(4-chlorophenyl)bismuth difluoride

Guidance literature:: In acetonitrile; stirred at room temp. for 1 h; filtered, concd., crystd. by addn. of hexane; elem. anal.;
DOI:10.1016/j.jorganchem.2004.07.055

Reference yield: 95.0%

: 13755-29-8
sodium tetrafluoroborate

: 121899-91-0
tris(4-chlorophenyl)bismuth difluoride

: 98-80-6
phenylboronic acid

: 214141-73-8
tris(4-chlorophenyl)phenylbismuthonium tetrafluoroborate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; water; stirring (room temp., 2 h), NaBF4 soln. (H2O) addn., stirring (30 min); extg. (CH2Cl2), drying (MgSO4), filtering, evapn. (reduced pressure), crystn. (Et2O / CH2Cl2 = 10 : 1);
DOI:10.1021/om9804531