C₄₈H₇₄N₂O₉Si₂

Base Information

Chemical Name:C₄₈H₇₄N₂O₉Si₂
CAS No.:1308253-71-5
Molecular Formula:C₄₈H₇₄N₂O₉Si₂
Molecular Weight:879.295
Hs Code.:

C<sub>48</sub>H<sub>74</sub>N<sub>2</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₄₈H₇₄N₂O₉Si₂

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Chemical Property of C₄₈H₇₄N₂O₉Si₂

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Technology Process of C₄₈H₇₄N₂O₉Si₂

There total 11 articles about C₄₈H₇₄N₂O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1308253-77-1
C₅₄H₈₈N₂O₉Si₃

: 1308253-71-5
C₄₈H₇₄N₂O₉Si₂

Guidance literature:: With formic acid; In tetrahydrofuran; water; at 20 ℃; for 2h;
DOI:10.1002/jhet.609

Reference yield:

: 1177255-27-4
(S)-methyl-2-acetamido-3-(3-formyl-4-methoxy-3-methylphenyl)propanoate

: 1308253-71-5
C₄₈H₇₄N₂O₉Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 6 h / 20 °C

2: hydrogenchloride; water / methanol / 10 h

3: lithium borohydride / tetrahydrofuran / 24 h

4: hydrogenchloride / methanol; water / 6 h / Reflux

5: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 9 h / -10 °C / Molecular sieve

6: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0 - 20 °C

7: triethylamine; trifluoroacetic acid / dichloromethane / 24 h / 20 °C

8: formic acid / tetrahydrofuran; water / 2 h / 20 °C

With hydrogenchloride; lithium borohydride; formic acid; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; 2,2,2-trifluoroethanol; water; 1: Baeyer-Villiger oxidation;
DOI:10.1002/jhet.609

Reference yield:

: 1177255-28-5
(S)-methyl-2-acetamido-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

: 1308253-71-5
C₄₈H₇₄N₂O₉Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: lithium borohydride / tetrahydrofuran / 24 h

2: hydrogenchloride / methanol; water / 6 h / Reflux

3: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 9 h / -10 °C / Molecular sieve

4: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0 - 20 °C

5: triethylamine; trifluoroacetic acid / dichloromethane / 24 h / 20 °C

6: formic acid / tetrahydrofuran; water / 2 h / 20 °C

With hydrogenchloride; lithium borohydride; formic acid; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; 2,2,2-trifluoroethanol; water;
DOI:10.1002/jhet.609