potassium β-{[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino}propionate

Base Information

Chemical Name:potassium β-{[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino}propionate
CAS No.:881690-76-2
Molecular Formula:C₁₂H₁₄NO₃*K
Molecular Weight:259.346
Hs Code.:

Synonyms:potassium β-{[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino}propionate

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Chemical Property of potassium β-{[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino}propionate

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Technology Process of potassium β-{[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino}propionate

There total 1 articles about potassium β-{[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 699-91-2
2-acetyl-6-methylphenol

: 107-95-9
3-amino propanoic acid

: 881690-76-2
potassium β-{[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino}propionate

Guidance literature:: With potassium hydroxide; In methanol; water; at 15 - 20 ℃; for 6h;
DOI:10.1016/j.jorganchem.2005.10.057

Reference yield: 65.0%

: 881690-76-2
potassium β-{[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino}propionate

: 1461-22-9
tributyltin chloride

: [Ph3Sn(β-[[(E)-1-(2-hydroxy-3-methylphenyl)ethylidene]amino]propionate)]

Guidance literature:: In chloroform; n-Bu3SnCl in anhyd. CHCl3 was added dropwise to stirred suspn. of ligandin CHCl3; mixt. stirred at ambient temp. for 6 h; filtered; filtrate evapd. at ambient temp.; residue triturated (hexane);filtered; ppt. washed (hexane); dried (vac.); recrystd. (hexane/CHCl3, 4:1); elem. anal.;
DOI:10.1016/j.jorganchem.2005.10.057