N,N-bis-[2-(2-aminoacetylamino)ethyl]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide

Base Information

Chemical Name:N,N-bis-[2-(2-aminoacetylamino)ethyl]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide
CAS No.:869339-46-8
Molecular Formula:C₁₇H₂₄I₃N₇O₄
Molecular Weight:771.136
Hs Code.:

Synonyms:N,N-bis-[2-(2-aminoacetylamino)ethyl]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide

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Chemical Property of N,N-bis-[2-(2-aminoacetylamino)ethyl]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide

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Technology Process of N,N-bis-[2-(2-aminoacetylamino)ethyl]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide

There total 2 articles about N,N-bis-[2-(2-aminoacetylamino)ethyl]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 869339-45-7
N,N-bis-[2-tert-butoxycarbonylaminoacetyl-(2-aminoethyl)]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide

: 869339-46-8
N,N-bis-[2-(2-aminoacetylamino)ethyl]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide

Guidance literature:: N,N-bis-[2-tert-butoxycarbonylaminoacetyl-(2-aminoethyl)]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide; With trifluoroacetic acid; at 20 ℃; for 3h;

With sodium hydroxide; In dichloromethane; water; pH=10;

Reference yield:

: 76350-18-0
2,4,6-triiodo-5-(methylamino)isophthaloyl dichloride

: 869339-46-8
N,N-bis-[2-(2-aminoacetylamino)ethyl]-5-(methylamino)-2,4,6-triiodoisophthalic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 15 h / 20 °C

2.1: trifluoroacetic acid / 3 h / 20 °C

2.2: pH 10

With triethylamine; trifluoroacetic acid; In tetrahydrofuran;