diethyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)hexanedioate

Base Information

Chemical Name:diethyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)hexanedioate
CAS No.:1132710-00-9
Molecular Formula:C₂₁H₃₁ClNO₇P
Molecular Weight:475.906
Hs Code.:

Synonyms:diethyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)hexanedioate

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Chemical Property of diethyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)hexanedioate

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Technology Process of diethyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)hexanedioate

There total 3 articles about diethyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)hexanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1132709-93-3
methyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)propanoate

: 140-88-5,9003-32-1
ethyl acrylate

: 1132710-00-9
diethyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)hexanedioate

Guidance literature:: methyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)propanoate; With sodium ethanolate; In ethanol; for 0.166667h;

ethyl acrylate; In ethanol; for 2h; Reflux;
DOI:10.1002/ejoc.200800812

Reference yield:

: 1132709-92-2
diethyl {[(3-chlorobenzylidene)amino]methyl}phosphonate

: 1132710-00-9
diethyl 3-[(3-chlorobenzylidene)amino]-3-(diethoxyphosphoryl)hexanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

2: sodium ethanolate / ethanol / 2 h / Reflux

With sodium ethanolate; lithium diisopropyl amide; In tetrahydrofuran; ethanol; 2: Michael condensation;
DOI:10.1007/s00726-010-0697-x