3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline

Base Information

Chemical Name:3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline
CAS No.:1314007-30-1
Molecular Formula:C₂₁H₂₂F₃NO₂Si
Molecular Weight:405.492
Hs Code.:

Synonyms:3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline

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Chemical Property of 3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline

Chemical Property:

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Technology Process of 3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline

There total 3 articles about 3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1314007-03-8
1-[2-(quinolin-3-yloxy)-phenyl]-ethanone

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 1314007-30-1
3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline

Guidance literature:: tetrabutyl ammonium fluoride; In tetrahydrofuran; for 4h; cooling with ice;

Reference yield:

: 580-18-7
3-hydroxyquinoline

: 1314007-30-1
3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; copper(l) chloride / 2,2,6,6-tetramethylheptane-3,5-dione / 1-methyl-pyrrolidin-2-one / 3 h / 130 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / cooling with ice

With caesium carbonate; copper(l) chloride; 2,2,6,6-tetramethylheptane-3,5-dione; tetrabutyl ammonium fluoride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;

Reference yield:

: 2142-69-0
2-bromophenyl methyl ketone

: 1314007-30-1
3-[2-(2,2,2-trifluoro-1-methyl-1-trimethylsilanyloxy-ethyl)-phenoxy]-quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; copper(l) chloride / 2,2,6,6-tetramethylheptane-3,5-dione / 1-methyl-pyrrolidin-2-one / 3 h / 130 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / cooling with ice

With caesium carbonate; copper(l) chloride; 2,2,6,6-tetramethylheptane-3,5-dione; tetrabutyl ammonium fluoride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;