C₅₂H₇₃NO₁₃Si₂

Base Information

Chemical Name:C₅₂H₇₃NO₁₃Si₂
CAS No.:172801-47-7
Molecular Formula:C₅₂H₇₃NO₁₃Si₂
Molecular Weight:976.322
Hs Code.:

C<sub>52</sub>H<sub>73</sub>NO<sub>13</sub>Si<sub>2</sub>

Synonyms:C₅₂H₇₃NO₁₃Si₂

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Chemical Property of C₅₂H₇₃NO₁₃Si₂

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Technology Process of C₅₂H₇₃NO₁₃Si₂

There total 5 articles about C₅₂H₇₃NO₁₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 162459-94-1
2'-(tert-butyldimethylsilyl)-2-debenzoyl-7-(triethylsilyl)paclitaxel

: 172801-47-7
C₅₂H₇₃NO₁₃Si₂

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jo951530u

Reference yield:

: 994-30-9
triethylsilyl chloride

: 172801-47-7
C₅₂H₇₃NO₁₃Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) imidazole, 2.) imidazole / 1) DMF, 60 deg C, 2 h; 2) DMF, rt, 1 h

2: 75 percent / benzyltrimethylammonium hydroxide / CH₂Cl₂ / 1) -78 deg C, 10 min; 2) -10 deg C, 10-15 min

3: 86 percent / tetrapropylammonium perruthenate, N-methylmorpholine N-oxide / CH₂Cl₂ / 3 h / Ambient temperature

With 1H-imidazole; tetrapropylammonium perruthennate; N-benzyl-trimethylammonium hydroxide; 4-methylmorpholine N-oxide; In dichloromethane;
DOI:10.1021/jo951530u

Reference yield:

: 33069-62-4
taxol

: 172801-47-7
C₅₂H₇₃NO₁₃Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) imidazole, 2.) imidazole / 1) DMF, 60 deg C, 2 h; 2) DMF, rt, 1 h

2: 75 percent / benzyltrimethylammonium hydroxide / CH₂Cl₂ / 1) -78 deg C, 10 min; 2) -10 deg C, 10-15 min

3: 86 percent / tetrapropylammonium perruthenate, N-methylmorpholine N-oxide / CH₂Cl₂ / 3 h / Ambient temperature

With 1H-imidazole; tetrapropylammonium perruthennate; N-benzyl-trimethylammonium hydroxide; 4-methylmorpholine N-oxide; In dichloromethane;
DOI:10.1021/jo951530u