4-(benzylthio)-3-fluorobenzoic acid

Base Information

Chemical Name:4-(benzylthio)-3-fluorobenzoic acid
CAS No.:1063733-08-3
Molecular Formula:C₁₄H₁₁FO₂S
Molecular Weight:262.305
Hs Code.:

Synonyms:4-(benzylthio)-3-fluorobenzoic acid

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Chemical Property of 4-(benzylthio)-3-fluorobenzoic acid

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Technology Process of 4-(benzylthio)-3-fluorobenzoic acid

There total 1 articles about 4-(benzylthio)-3-fluorobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 455-86-7
3,4-Difluorobenzoic acid

: 100-53-8
phenylmethanethiol

: 1063733-08-3
4-(benzylthio)-3-fluorobenzoic acid

Guidance literature:: 3,4-Difluorobenzoic acid; phenylmethanethiol; With caesium carbonate; In dimethyl sulfoxide; at 70 ℃; for 3h;

With hydrogenchloride; In water; pH=1;

Reference yield:

: 67-56-1
methanol

: 1063733-08-3
4-(benzylthio)-3-fluorobenzoic acid

: 1219687-19-0
methyl 4-(benzylthio)-3-fluorobenzoate

Guidance literature:: With sulfuric acid; for 36h; Reflux;

Reference yield:

: 1063733-08-3
4-(benzylthio)-3-fluorobenzoic acid

: 1219687-06-5
N-[3-chloro-4-(trifluoromethoxy)benzyl]-3-fluoro-4-[(1,3-thiazol-2-ylamino)sulfonyl]benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 36 h / Reflux

2: hydrogenchloride; sodium hypochlorite / water; dichloromethane / 5 - 20 °C

3: pyridine / 18 h / 50 °C

4: lithium hydroxide / water; 1,4-dioxane / 4.5 h / 5 - 20 °C

5: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dimethyl sulfoxide / 18 h / 20 °C

With hydrogenchloride; sodium hypochlorite; sulfuric acid; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; lithium hydroxide; In 1,4-dioxane; pyridine; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1039/c7md00131b