aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate

Base Information

Chemical Name:aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate
CAS No.:609810-33-5
Molecular Formula:BF₄*C₂₁H₁₇F₁₂N₂OPd
Molecular Weight:734.584
Hs Code.:

Synonyms:aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate

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Chemical Property of aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate

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Technology Process of aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate

There total 2 articles about aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 400608-66-4
N,N’-bis-(3,5di(trifluoromethyl)phenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

: 609810-33-5
aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: water

In diethyl ether; water;
DOI:10.1021/om0303294

Reference yield:

: tetrafluoroboric acid

: 609810-40-4
[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]dimethylpalladium(II)

: 7732-18-5
water

: 609810-33-5
aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate

Guidance literature:: In water; dry trifluoroethanol-d3 added to NMR tube contg. the Pd complex; aq. HBF4 added; mixt. shaken to form clear soln.; not isolated; NMR anal.;
DOI:10.1021/om0303294

Reference yield:

: 609810-33-5
aqua[1,4-bis(3,5-ditrifluoromethylphenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene]methylpalladium(II) tetrafluoroborate

: 7440-05-3
palladium

Guidance literature:: With benzene; In water; byproducts: methane, biphenyl; under inert atmosphere; in NMR tube; benzene added to soln. of the Pd complex in aq. trifluoroethanol-d3; at room temp.; NMR anal.;
DOI:10.1021/om0303294