ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride

Base Information

• Chemical Name: ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride
• CAS No.: 108967-17-5
• Molecular Formula: C₁₅H₁₉NO₅S*ClH
• Molecular Weight: 361.846
• Mol file: 108967-17-5.mol

Synonyms:ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride

Chemical Property of ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride

There total 1 articles about ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

5-O-benzoyl-β-D-ribofuranosyl cyanide (30002-87-0) + ethanethiol (75-08-1) → ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride (108967-17-5)

Guidance literature:

With hydrogenchloride; In diethyl ether; at 0 ℃;

DOI:10.1016/S0008-6215(00)90269-6

Reference yield: 82.0%

ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride (108967-17-5) → ethyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate (108967-20-0)

Guidance literature:

With hydrogen sulfide; In pyridine; at 0 ℃;

DOI:10.1016/S0008-6215(00)90269-6

Reference yield: 9.0%

5,6-Diamino-1,3-dimethyluracil hydrate + ethyl 2,5-anhydro-6-O-benzoyl-D-allonothioimidate hydrochloride (108967-17-5) → 8-(5-O-benzoyl-β-D-ribofuranosyl)-1,3-dimethylxanthine (108967-26-6)

Guidance literature:

With pyridine; for 2h; Heating;

DOI:10.1016/S0008-6215(00)90269-6

upstream raw materials:

5-O-benzoyl-β-D-ribofuranosyl cyanide

ethanethiol

Downstream raw materials:

8-(5-O-benzoyl-β-D-ribofuranosyl)-1,3-dimethylxanthine

ethyl 2,5-anhydro-6-O-benzoyl-D-allonodithioate

2-(5-O-benzoyl-β-D-ribofuranosyl)benzoxazole

1,3-dimethyl-8-β-D-ribofuranosylxanthine