C₃₇H₆₀O₄Si

Base Information

Chemical Name:C₃₇H₆₀O₄Si
CAS No.:1353388-71-2
Molecular Formula:C₃₇H₆₀O₄Si
Molecular Weight:596.966
Hs Code.:

C<sub>37</sub>H<sub>60</sub>O<sub>4</sub>Si

Synonyms:C₃₇H₆₀O₄Si

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Chemical Property of C₃₇H₆₀O₄Si

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Technology Process of C₃₇H₆₀O₄Si

There total 10 articles about C₃₇H₆₀O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1344148-95-3
(R)-5-(tert-butyldiphenylsilyloxy)-1,1-diethoxyheptadec-2-yn-4-ol

: 1353388-71-2
C₃₇H₆₀O₄Si

Guidance literature:: With hydrogen; In hexane; at 20 ℃; for 0.916667h;
DOI:10.1016/j.tetlet.2011.08.160

Reference yield:

: 1344148-85-1
(R)-methyl 4-(tert-butyldimethylsilyloxy)-2-(tert-butyldiphenylsilyloxy)butanoate

: 1353388-71-2
C₃₇H₆₀O₄Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 7 h / -78 °C

2.1: pyridine; dmap / 3 h / 0 - 20 °C

3.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 7 h / 0 - 20 °C

4.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 6 h / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

5.2: 0.17 h / 0 °C

6.1: palladium 10% on activated carbon; hydrogen / methanol / 41 h / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

8.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 8 h / 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 0 °C

9.2: 0.67 h / -78 - 20 °C

10.1: hydrogen / hexane / 0.92 h / 20 °C

With pyridine; dmap; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; 5.1: Wittig reaction / 5.2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.08.160

Reference yield:

: 1344148-86-2
(R)-4-(tert-butyldimethylsilyloxy)-2-(tert-butyldiphenylsilyloxy)butan-1-ol

: 1353388-71-2
C₃₇H₆₀O₄Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine; dmap / 3 h / 0 - 20 °C

2.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 7 h / 0 - 20 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 6 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

4.2: 0.17 h / 0 °C

5.1: palladium 10% on activated carbon; hydrogen / methanol / 41 h / 20 °C

6.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

7.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 8 h / 20 °C

8.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 0 °C

8.2: 0.67 h / -78 - 20 °C

9.1: hydrogen / hexane / 0.92 h / 20 °C

With pyridine; dmap; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; 4.1: Wittig reaction / 4.2: Wittig reaction;
DOI:10.1016/j.tetlet.2011.08.160