2-(7-Methoxynaphthalen-1-yl)acetyl chloride

Base Information

Chemical Name:2-(7-Methoxynaphthalen-1-yl)acetyl chloride
CAS No.:6836-23-3
Molecular Formula:C₁₃H₁₁ClO₂
Molecular Weight:234.682
Hs Code.:2914790090
DSSTox Substance ID:DTXSID301283006

Synonyms:6836-23-3;2-(7-methoxynaphthalen-1-yl)acetyl chloride;(7-Methoxy-1-naphthyl)acetyl chloride;1-Naphthaleneacetyl chloride, 7-methoxy-;(7-methoxy-naphthalen-1-yl)-acetyl chloride;(7-methoxy-1-naphthyl)acetic acid chloride;SCHEMBL4753009;CRIAVNMNHHQBGQ-UHFFFAOYSA-N;DTXSID301283006;MFCD27956331;(7-Methoxynaphth-1-yl)acetyl chloride;7-Methoxy-1-naphthaleneacetyl chloride;2-(7-methoxynaphthalen-1-yl)acetylchloride;DB-344802

Suppliers and Price of 2-(7-Methoxynaphthalen-1-yl)acetyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Atlantic Research Chemicals
(7-Methoxy-1-naphthyl)acetylchloride 95%
5gm:
$ 1123.99

Advanced Chemicals Intermediatesced Chemicals Intermediates
(7-Methoxy-naphthalen-1-yl)-acetylchloride 95%+
10g
$ 1732.75

Acints
(7-Methoxy-naphthalen-1-yl)-acetylchloride 95%+
10g
$ 1732.75

Acints
(7-Methoxy-naphthalen-1-yl)-acetylchloride 95%+
5g
$ 978.75

Acints
(7-Methoxy-naphthalen-1-yl)-acetylchloride 95%+
1g
$ 282.75

Total 3 raw suppliers

Chemical Property of 2-(7-Methoxynaphthalen-1-yl)acetyl chloride

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:234.0447573
Heavy Atom Count:16
Complexity:254

Purity/Quality:

99%, ^*data from raw suppliers

(7-Methoxy-1-naphthyl)acetylchloride 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=C(C=CC=C2CC(=O)Cl)C=C1

Technology Process of 2-(7-Methoxynaphthalen-1-yl)acetyl chloride

There total 6 articles about 2-(7-Methoxynaphthalen-1-yl)acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 6836-22-2
2-(7-methoxynaphthalen-1-yl)acetic acid

: 6836-23-3
(7-methoxy-1-naphthyl)acetic acid chloride

Guidance literature:: With thionyl chloride; In dichloromethane; N,N-dimethyl-formamide; at 35 - 40 ℃;

Reference yield:

: 6836-19-7
7-Methoxy-1-tetralone

: 6836-23-3
(7-methoxy-1-naphthyl)acetic acid chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: zinc / iodine / toluene / Reflux

1.2: Reflux

1.3: 3 h / Reflux

2.1: sulfur / ethyl acetate / 10 h / 215 °C

3.1: sodium hydroxide; water / ethanol / 3 h / 20 °C

4.1: thionyl chloride / dichloromethane / 2 h / Reflux

With thionyl chloride; water; sulfur; sodium hydroxide; zinc; iodine; In ethanol; dichloromethane; ethyl acetate; toluene;

Reference yield:

: 6836-21-1
ethyl 2-(7-methoxynaphthalen-1-yl)acetate

: 6836-23-3
(7-methoxy-1-naphthyl)acetic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / ethanol / 3 h / 20 °C

2: thionyl chloride / dichloromethane / 2 h / Reflux

With thionyl chloride; water; sodium hydroxide; In ethanol; dichloromethane;