4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

Base Information

Chemical Name:4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester
CAS No.:476192-19-5
Molecular Formula:C₂₁H₃₀O₈S
Molecular Weight:442.53
Hs Code.:

Synonyms:4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

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Chemical Property of 4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

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Technology Process of 4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

There total 4 articles about 4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 476192-17-3
C₂₁H₃₂O₇S

: 476192-19-5
4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

Guidance literature:: With sodium periodate; ruthenium trichloride; In tetrachloromethane; water; acetonitrile; for 1h;

Reference yield:

: 476192-12-8
4-[(4-fluorophenyl)sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

: 476192-19-5
4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / 4 h / 0 - 20 °C

2: 5% Pd(II)/C(eggshell) / tetrahydrofuran / 1.5 h / 4137.29 Torr

3: sodium periodate; ruthenium trichloride / tetrachloromethane; water

With ruthenium trichloride; sodium periodate; 5% Pd(II)/C(eggshell); sodium hydride; In tetrahydrofuran; tetrachloromethane; water;
DOI:10.1016/j.bmcl.2011.03.095

Reference yield:

: 1310544-18-3
C₂₈H₃₈O₇S

: 476192-19-5
4-[[4-(4-carboxybutoxy)phenyl-]sulfonyl]tetrahydro-2H-pyran-4-carboxylic acid, 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 5% Pd(II)/C(eggshell) / tetrahydrofuran / 1.5 h / 4137.29 Torr

2: sodium periodate; ruthenium trichloride / tetrachloromethane; water

With ruthenium trichloride; sodium periodate; 5% Pd(II)/C(eggshell); In tetrahydrofuran; tetrachloromethane; water;
DOI:10.1016/j.bmcl.2011.03.095